Molecular mass determination of polyamic acid ionic salt by size-exclusion chromatography

P. Santhana Gopala Krishnan, S. Veeramani, Rohit H. Vora*, Tai Shung Chung, Shun Ichiro Uchimura, Hatsuo Sugitani

*Corresponding author for this work

Research output: Contribution to journalArticlepeer-review

9 Scopus citations

Abstract

A methodology was developed for the determination of molecular weight averages of polyamic acid ionic salt (PAS) by size-exclusion chromatography (SEC). Polystyrene standards were used for calibration and THF-DMF 1:1 by volume containing 0.06 M LiBr and 0.06 M H3PO4 was used as the mobile phase. The proposed methodology was found to be reproducible.

Original languageEnglish (US)
Pages (from-to)207-212
Number of pages6
JournalJournal of Chromatography A
Volume977
Issue number2
DOIs
StatePublished - Nov 22 2002
Externally publishedYes

Keywords

  • Molecular mass determination
  • Polyamic acid ionic salt

ASJC Scopus subject areas

  • Analytical Chemistry
  • Biochemistry
  • Organic Chemistry

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