Effects of low-temperature carbonization temperature and time on morphology of carbon particles from maize starch

Zhonghua Xue; Peirong Chen; Qi Yang; Lifang He; Shuhui Mu; Beijiu Cheng

doi:10.1007/s10853-013-7911-7

Effects of low-temperature carbonization temperature and time on morphology of carbon particles from maize starch

Zhonghua Xue, Peirong Chen^*, Qi Yang, Lifang He, Shuhui Mu, Beijiu Cheng

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

11 Scopus citations

Abstract

Carbon particles retaining the morphology of native maize starch were prepared successfully in nitrogen by low-temperature carbonization (LTC) treatment and subsequent carbonization at 600 °C for 1 h. The as-prepared carbon particles were characterized by FESEM and the process of LTC was investigated by XRD, FTIR, DSC, TGA, and elemental analysis. The results indicate that the LTC treatment is mainly the process of starch dehydration and the LTC condition has crucial effects on the morphology of final carbon particles. When the maize starch was treated with proper LTC process, the carbon content of treated maize starch is more than 51 %, and the final carbon particles show good dispersity.

Original language	English (US)
Pages (from-to)	2180-2186
Number of pages	7
Journal	Journal of Materials Science
Volume	49
Issue number	5
DOIs	https://doi.org/10.1007/s10853-013-7911-7
State	Published - Mar 2014

Bibliographical note

Funding Information:
Acknowledgements The authors would like to thank the Natural Science Foundation of Anhui Provincial Education Department (KJ2012Z104), National University Students Innovation Project of China (201210364027) and 973 Program of China (2014CB138200) for financial support.

ASJC Scopus subject areas

General Materials Science
Mechanics of Materials
Mechanical Engineering

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title = "Effects of low-temperature carbonization temperature and time on morphology of carbon particles from maize starch",

abstract = "Carbon particles retaining the morphology of native maize starch were prepared successfully in nitrogen by low-temperature carbonization (LTC) treatment and subsequent carbonization at 600 °C for 1 h. The as-prepared carbon particles were characterized by FESEM and the process of LTC was investigated by XRD, FTIR, DSC, TGA, and elemental analysis. The results indicate that the LTC treatment is mainly the process of starch dehydration and the LTC condition has crucial effects on the morphology of final carbon particles. When the maize starch was treated with proper LTC process, the carbon content of treated maize starch is more than 51 %, and the final carbon particles show good dispersity.",

author = "Zhonghua Xue and Peirong Chen and Qi Yang and Lifang He and Shuhui Mu and Beijiu Cheng",

note = "Funding Information: Acknowledgements The authors would like to thank the Natural Science Foundation of Anhui Provincial Education Department (KJ2012Z104), National University Students Innovation Project of China (201210364027) and 973 Program of China (2014CB138200) for financial support.",

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doi = "10.1007/s10853-013-7911-7",

language = "English (US)",

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T1 - Effects of low-temperature carbonization temperature and time on morphology of carbon particles from maize starch

AU - Xue, Zhonghua

AU - Chen, Peirong

AU - Yang, Qi

AU - He, Lifang

AU - Mu, Shuhui

AU - Cheng, Beijiu

N1 - Funding Information: Acknowledgements The authors would like to thank the Natural Science Foundation of Anhui Provincial Education Department (KJ2012Z104), National University Students Innovation Project of China (201210364027) and 973 Program of China (2014CB138200) for financial support.

PY - 2014/3

Y1 - 2014/3

N2 - Carbon particles retaining the morphology of native maize starch were prepared successfully in nitrogen by low-temperature carbonization (LTC) treatment and subsequent carbonization at 600 °C for 1 h. The as-prepared carbon particles were characterized by FESEM and the process of LTC was investigated by XRD, FTIR, DSC, TGA, and elemental analysis. The results indicate that the LTC treatment is mainly the process of starch dehydration and the LTC condition has crucial effects on the morphology of final carbon particles. When the maize starch was treated with proper LTC process, the carbon content of treated maize starch is more than 51 %, and the final carbon particles show good dispersity.

AB - Carbon particles retaining the morphology of native maize starch were prepared successfully in nitrogen by low-temperature carbonization (LTC) treatment and subsequent carbonization at 600 °C for 1 h. The as-prepared carbon particles were characterized by FESEM and the process of LTC was investigated by XRD, FTIR, DSC, TGA, and elemental analysis. The results indicate that the LTC treatment is mainly the process of starch dehydration and the LTC condition has crucial effects on the morphology of final carbon particles. When the maize starch was treated with proper LTC process, the carbon content of treated maize starch is more than 51 %, and the final carbon particles show good dispersity.

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Effects of low-temperature carbonization temperature and time on morphology of carbon particles from maize starch

Abstract

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