Abstract
Ultrafiltration asymmetric porous membranes were imaged by two microscopy methods, which allow 3D reconstruction: Focused Ion Beam and Serial Block Face Scanning Electron Microscopy. A new algorithm was proposed to evaluate porosity and average pore size in different layers orthogonal and parallel to the membrane surface. The 3D-reconstruction enabled additionally the visualization of pore interconnectivity in different parts of the membrane. The method was demonstrated for a block copolymer porous membrane and can be extended to other membranes with application in ultrafiltration, supports for forward osmosis, etc, offering a complete view of the transport paths in the membrane.
Original language | English (US) |
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Pages (from-to) | 3689-3695 |
Number of pages | 7 |
Journal | Industrial & Engineering Chemistry Research |
Volume | 55 |
Issue number | 12 |
DOIs | |
State | Published - Mar 21 2016 |
Bibliographical note
KAUST Repository Item: Exported on 2020-10-01Acknowledgements: This work was supported by the King Abdullah University of Science and Technology
(KAUST), KAUST Project “Visualization and Pore Tuning of Asymmetric Membranes”.